反应条件
in N,N-dimethyl-formamide; acetonitrile byproducts: sulfur; oxomolybdate dissolved in CH3CN, addn. (2-3 min) of ferrocenium dissolved in DMF, stirring (5 min), concn. (-196°C, 0.1 Torr), filtration in vac., addn. of propanol, keeping at 0°C (12 h); filtration, washing (diethyl ether), recrystn. (MeCN/2-propanol) at 0°C; elem. anal., powder X-ray diffraction;
参考文献
Hadjikyriacou, A. I.; Coucouvanis, D.
Inorganic Chemistry, 1989 , vol. 28, p. 2169 - 2177
