1: benzyl-methyl-amine With REM resin T=20°C; 3 h; 2: benzyl bromide in N,N-dimethyl-formamide 18 h; 3: With N-ethyl-N,N-diisopropylamine in dichloromethane
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zinc(II) tetrahydroborate; zinc(II) chloride in tetrahydrofuran 8 h; Ambient temperatureN-methylation of aliphatic and aromatic primarily and secondary amines with paraformaldehyde in the presence of zinc chloride and zinc borohydride to tertiary methylated amines; Product distribution;
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3 platinum on carbon; hydrogen in toluene T=105°C; P=4500.45 Torr; Flow reactor;
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Sharma, Sumeet K.; Lynch, James; Sobolewska, Anna M.; Plucinski, Pawel; Watson, Robert J.; Williams, Jonathan M. J.
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