2,2-二乙氧基乙基 苯甲酸合成路线 (共 6 条)
反应条件
in pyridine T=-20 - 30°C; 167.833 h;
参考文献
Eisai Co., Ltd.
Patent: US2007/10542 A1, 2007 ;
Location in patent: Page/Page column 95 ;
反应条件
potassium iodide in N,N-dimethyl-formamide 20 h; Heating / reflux; Product distribution / selectivity;
参考文献
Daicel Chemical Industries, Ltd.
Patent: US2005/234246 A1, 2005 ;
Location in patent: Page/Page column 4 ;
反应条件
in N,N-dimethyl-formamide 5 h; Heating;
参考文献
THESIS CHEMISTRY, LLC
Patent: US2012/157693 A1, 2012 ;
Location in patent: Page/Page column 9 ;
反应条件
potassium carbonate; potassium iodide in N,N-dimethyl-formamide 20 h; Heating / reflux; Product distribution / selectivity;
参考文献
Daicel Chemical Industries, Ltd.
Patent: US2005/234246 A1, 2005 ;
Location in patent: Page/Page column 4 ;
反应条件
1: aqueous KOH-solution / 120 °C 2: aqueous KOH View Scheme
参考文献
Gryszkiewicz-Trochimowski et al.
Bulletin de la Societe Chimique de France, 1958 , p. 610,615
反应条件
formic acid T=20°C; 3 h;
参考文献
Du, Jinfa; Watanabe, Kyoichi A.
Synthetic Communications, 2004 , vol. 34, # 11 p. 1925 - 1930