2,6-二氯醌-4-氯亚胺合成路线 （共 19 条）
反应条件
Na2B4O7 in acetonitrile T=25°C; 0.0666667 h; Title compound not separated from byproducts;
参考文献
Pallagi, Istvan; Toro, Andras; Farkas, Oedoen
Journal of Organic Chemistry, 1994 , vol. 59, # 22 p. 6543 - 6557
反应条件
hydrogenchloride; sodium hydroxide; sodium periodate; Na2S2O4 in tetrahydrofuran; methanol; water; ethyl acetate; DDAO
参考文献
MILES INC.
Patent: EP324912 A3, 1990 ;
反应条件
hydrogenchloride 3.08333 h; decomposition; Rate constant;
参考文献
El-Kholy, Aly E.; Harfoush, Aly A.; Kasem, Taher S.; Fathalla, Magda F.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, # 2 p. 137 - 139
反应条件
hydrogenchloride; sodium hydroxide; sodium periodate; Na2S2O4 in tetrahydrofuran; methanol; water; ethyl acetate; DDAO
参考文献
MILES INC.
Patent: EP324912 A3, 1990 ;
反应条件
1: 2M NaOH / tetrahydrofuran; H2O / 1.5 h / 0 °C 2: Na2S2O4 / ethyl acetate; H2O 3: 2M HCl / methanol / 1.25 h / 100 °C 4: 82 percent / NaIO3 / H2O; ethyl acetate / 0.25 h View Scheme
参考文献
Corey, Paul F.; Trimmer, Robert W.; Biddlecom, William G.
Angewandte Chemie, 1991 , vol. 103, # 12 p. 1694 - 1696
反应条件
in pyridine Gibbs test; Mechanism;
参考文献
Nagarajan; Rani; Parmar
Pharmazie, 1983 , vol. 38, # 1 p. 72 - 73
反应条件
p-benozquinone in acetonitrile-D3; water-d2 T=25°C; Gibbs reaction; pH=9.2; 0.25 h; Product distributionKinetics; Further Variations:Reagents;
参考文献
Pallagi, Istvan; Toro, Andras; Horvath, Gyula
Journal of Organic Chemistry, 1999 , vol. 64, # 18 p. 6530 - 6540
反应条件
1: 2M NaOH / tetrahydrofuran; H2O / 1.5 h / 0 °C 2: Na2S2O4 / ethyl acetate; H2O 3: 2M HCl / methanol / 1.25 h / 100 °C 4: 82 percent / NaIO3 / H2O; ethyl acetate / 0.25 h 5: 1M NaOH, H2 / Raney nickel / ethyl acetate / 5 h / 70 °C / 2067.2 Torr 6: NaIO4 / ethyl acetate; H2O / 0.17 h / Ambient temperature View Scheme
参考文献
Corey, Paul F.; Trimmer, Robert W.; Biddlecom, William G.
Angewandte Chemie, 1991 , vol. 103, # 12 p. 1694 - 1696
反应条件
Na2B4O7; oxygen in acetonitrile
T=25°C; Title compound not separated from byproducts;
参考文献
Pallagi, Istvan; Toro, Andras; Farkas, Oedoen
Journal of Organic Chemistry, 1994 , vol. 59, # 22 p. 6543 - 6557
