N-(2-氨基乙基)苯甲酰胺合成路线 （共 22 条）
参考文献
Hill; Aspinall
Journal of the American Chemical Society, 1939 , vol. 61, p. 822,824
反应条件
hydrogen; palladium on activated charcoal in ethanol
P=3102.9 Torr; 24 h;
参考文献
Barker, Peter L.; Gendler, Paul L.; Rapoport, Henry
Journal of Organic Chemistry, 1981 , vol. 46, # 12 p. 2455 - 2465
反应条件
1:
2: With trifluoroacetic acid in dichloromethane
12 h;
参考文献
Wiget, Paul A.; Manzano, Lawrence A.; Pruet, Jeff M.; Gao, Grace; Saito, Ryota; Monzingo, Arthur F.; Jasheway, Karl R.; Robertus, Jon D.; Anslyn, Eric V.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 24 p. 6799 - 6804
反应条件
palladium 10 on activated carbon; hydrogen in methanol
T=20°C; P=750.075 Torr;
参考文献
Gutmann, Bernhard; Roduit, Jean-Paul; Roberge, Dominique; Kappe, C. Oliver
Chemistry - A European Journal, 2011 , vol. 17, # 47 p. 13146 - 13150
反应条件
1: ethylenediamine With 9-borabicyclo[3.3.1]nonane dimer in tetrahydrofuran; hexane
T=20°C; 1 h;
2: benzoyl chloride in tetrahydrofuran; hexane
T=20°C; 2 h;
参考文献
Zhang, Zhongxing; Yin, Zhiwei; Meanwell, Nicholas A.; Kadow, John F.; Wang, Tao
Organic Letters, 2003 , vol. 5, # 19 p. 3399 - 3402
反应条件
trifluoroacetic acid in dichloromethane
参考文献
NOGRA PHARMA LIMITED; HOMMES, Daan; VERHAAR, Auke; VAN DEN BRINK, Gijs; VITI, Francesa
Patent: WO2013/178816 A1, 2013 ;
Location in patent: Paragraph 00152; 00153 ;
反应条件
in ethanol; water
T=20°C; 6.16667 h;
参考文献
Verma, Sanjeev K.; Acharya; Kaushik
Organic Letters, 2010 , vol. 12, # 19 p. 4232 - 4235
反应条件
lithium bromide
T=20°C;
参考文献
Abaee, M. Saeed; Akbarzadeh, Elahe; Sharifi, Roholah; Mojtahedi, Mohammad M.
Monatshefte fur Chemie, 2010 , vol. 141, # 7 p. 757 - 761
反应条件
1: 88 percent / triethylamine / diethyl ether
2: 740 mg / H2 / 10percent Pd/C / ethanol / 24 h / 3102.9 Torr
View Scheme
参考文献
Barker, Peter L.; Gendler, Paul L.; Rapoport, Henry
Journal of Organic Chemistry, 1981 , vol. 46, # 12 p. 2455 - 2465
反应条件
in tetrahydrofuran
T=25°C; 14 h; Inert atmosphere;
参考文献
Li, Hong; Pang, Zi-Bo; Jiao, Zhi-Feng; Lin, Fei
Journal of Combinatorial Chemistry, 2010 , vol. 12, # 2 p. 255 - 259
