5-甲基-3-苯基异噁唑合成路线 (共 67 条)
反应条件
1: With TsNHOH; potassium carbonate in methanol; water T=40°C; 24 h; 2: With potassium carbonate in methanol; water T=60°C; 10 h; regiospecific reaction;
参考文献
Tang, Shibing; He, Jinmei; Sun, Yongquan; He, Liuer; She, Xuegong
Organic Letters, 2009 , vol. 11, # 17 p. 3982 - 3985
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine; p-toluenesulfonyl chloride in acetonitrile T=0 - 20°C; 4 h;
参考文献
Tang, Shibing; He, Jinmei; Sun, Yongquan; He, Liuer; She, Xuegong
Journal of Organic Chemistry, 2010 , vol. 75, # 6 p. 1961 - 1966
参考文献
v. Auwers; Mueller
Journal fuer Praktische Chemie (Leipzig), 1933 , vol. <2> 137, p. 102,128
反应条件
N-chloro-succinimide; triethylamine in ethyl acetate; N,N-dimethyl-formamide
参考文献
WARNER-LAMBERT COMPANY
Patent: EP245825 B1, 1991 ;
反应条件
copper(l) iodide; 1,10-phenanthroline in o-xylene T=150°C; 6 h; Inert atmosphere;
参考文献
Nakatani, Yuji; Koizumi, Yuichiro; Yamasaki, Ryu; Saito, Shinichi
Organic Letters, 2008 , vol. 10, # 10 p. 2067 - 2070
反应条件
potassium carbonate in methanol T=25°C; 12 h;
参考文献
Short; Ziegler Jr.
Tetrahedron Letters, 1993 , vol. 34, # 1 p. 75 - 78
反应条件
potassium carbonate in methanol Ambient temperature;
参考文献
Short; Ziegler Jr.
Tetrahedron Letters, 1993 , vol. 34, # 1 p. 75 - 78
反应条件
disodium hydrogenphosphate; sodium amalgam in methanol 2 h;
参考文献
Yokoyama, Masataka; Tsuji, Kouichi; Kushida, Mari
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 67 - 72
反应条件
sodium hydroxide in ethanol 48 h; Ambient temperature;
参考文献
Dzierkacz, Irena M.; Kostka, Krzysztof
Polish Journal of Chemistry, 1985 , vol. 59, # 2 p. 177 - 187
反应条件
sodium hydroxide; hydroxylamine hydrochloride in ethanol 2 h; Heating;
参考文献
Kashima, Choji; Katoh, Akira; Yokota, Yuko; Omote, Yoshimori
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 9 p. 2516 - 2519