1007476-32-5合成路线 (共 278 条)
参考文献
Hagemann
Chemische Berichte, vol. 26, p. 876
反应条件
1: NaCH(CO2Et)COCH3 With n-butyllithium in tetrahydrofuran; hexane T=0°C; 0.75 h; Inert atmosphere; 2: (E,E)-3,7,11-trimethyl-2,6,10-dodecatrienyl bromide in tetrahydrofuran; hexane T=0°C; Inert atmosphere; 3: With dipotassium hydrogenphosphate in tetrahydrofuran; hexane
参考文献
Duez, Stephanie; Coudray, Laetitia; Mouray, Elisabeth; Grellier, Philippe; Dubois, Joelle
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 2 p. 543 - 556
反应条件
diethyl ether Behandlung des Reaktionsprodukts mit Natriummethylat-Loesung;
参考文献
Staellberg-Stenhagen
Arkiv foer Kemi, 1946 , vol. 20 A, # 19 p. 5,7, 12
参考文献
Matsukawa
Yakugaku Zasshi, 1942 , vol. 62, p. 417,443;dtsch.Ref.S.122,125
Chem.Abstr., 1951 , p. 4724
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Willimann; Schinz
Helvetica Chimica Acta, 1952 , vol. 35, p. 2401,2405
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Knunjanz; Tschelinzew; Ossetrowa
Doklady Akademii Nauk SSSR, 1934 , p. I 314
Chem. Zentralbl., 1934 , vol. 105, # II p. 2381
参考文献
Matsukawa
Yakugaku Zasshi, 1942 , vol. 62, p. 417,443;dtsch.Ref.S.122,125
Chem.Abstr., 1951 , p. 4724
参考文献
Knunjanz; Tschelinzew; Ossetrowa
Doklady Akademii Nauk SSSR, 1934 , p. I 314
Chem. Zentralbl., 1934 , vol. 105, # II p. 2381
反应条件
ethanol und Erhitzen des Reaktionsprodukts mit wss.-aethanol.Natronlauge;
参考文献
Isler et al.
Helvetica Chimica Acta, 1956 , vol. 39, p. 897,902
Helvetica Chimica Acta, 1958 , vol. 41, p. 786,788
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Dicker; Whitting
Journal of the Chemical Society, 1958 , p. 1994,1999
反应条件
ethanol und Erhitzen des Reaktionsprodukts mit wss.-aethanol.Natronlauge;
参考文献
Isler et al.
Helvetica Chimica Acta, 1956 , vol. 39, p. 897,902
Helvetica Chimica Acta, 1958 , vol. 41, p. 786,788
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Dicker; Whitting
Journal of the Chemical Society, 1958 , p. 1994,1999
参考文献
Barnett; Cook; Matthews
Journal of the Chemical Society, 1923 , vol. 123, p. 2005
反应条件
in tetrahydrofuran Stirring (room temp., 15 h).; Extg. (ether), washing of ext. (aq. HCl, H2O), drying (Na2SO4), evapn. of solvent in vac., chromy. (hexane-ethyl acetate), elem. anal.;
参考文献
Itoh, Keiji; Nakanishi, Saburo; Otsuji, Yoshio
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 10 p. 2965 - 2977