氢溴化N-(2-溴乙基)苯胺合成路线 （共 9 条）
反应条件
sodium hydroxide in ethanol 4 h;
参考文献
Sohar,P. et al.
Journal of Heterocyclic Chemistry, 1969 , vol. 6, p. 163 - 174
参考文献
Doherty et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 5667,5670
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Bergmann; Kaluszyner
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 289,309
反应条件
sodium hydroxide; ethanol
参考文献
Heine et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 1173
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Heine; Kapur
Journal of the American Chemical Society, 1955 , vol. 77, p. 4892
反应条件
1: 82.1 percent / ethanol / 4 h / Heating
2: 2.4 g / benzene / 3 h / Heating
3: 22.9 percent / diethyl ether
View Scheme
参考文献
Okada; Shimabayashi
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 11 p. 3310 - 3314
反应条件
1: 87.6 percent / ethanol / 4 h / Heating
2: benzene / 3 h / Heating
3: 21.1 percent / diethyl ether
View Scheme
参考文献
Okada; Shimabayashi
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 11 p. 3310 - 3314
反应条件
1: 65 percent / ethanol / 4 h / Heating
2: benzene / 3 h / Heating
3: 21.1 percent / diethyl ether
View Scheme
参考文献
Okada; Shimabayashi
Chemical and Pharmaceutical Bulletin, 1980 , vol. 28, # 11 p. 3310 - 3314
反应条件
in methanol
1) boiling, 1.5 h, 2) r.t., overnight;
参考文献
Lobanov, P. S.; Solod, O. V.; Potekhin, A. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , p. 2017 - 2021
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 11 p. 2310 - 2315
反应条件
2: aqueous NaOH
View Scheme
参考文献
Bergmann; Kaluszyner
Recueil des Travaux Chimiques des Pays-Bas, 1959 , vol. 78, p. 289,309
参考文献
Heine et al.
Journal of the American Chemical Society, 1954 , vol. 76, p. 1173
