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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1005-62-5
合成路线
（共 10 条）
18800-34-5
1-(2-溴乙氧基)-4-甲基苯
→
反应条件
1005-62-5
反应条件
sodium hydroxide T=250 - 300°C;
参考文献
Powell; Adams
Journal of the American Chemical Society, 1920 , vol. 42, p. 655
106-44-5
对甲酚
→
反应条件
1005-62-5
反应条件
potassium hydroxide; acetylene T=185°C;
参考文献
Schosstakowsski; Burmisstrowa
Zhurnal Prikladnoi Khimii (Sankt-Peterburg, Russian Federation), 1942 , vol. 15, p. 260
Chem.Abstr., 1943 , p. 2337
106-44-5
对甲酚
+
1119-20-6
二乙烯基汞
→
反应条件
1005-62-5
反应条件
T=100°C; 3 h;
参考文献
Foster,D.J.; Tobler,E.
Journal of the American Chemical Society, 1961 , vol. 83, p. 851 - 855
106-44-5
对甲酚
+
106-93-4
二溴乙烷
→
反应条件
1005-62-5
反应条件
(i) NaOH, (ii) KOtBu, DMSO; Multistep reaction;
参考文献
McClelland,R.A.
Canadian Journal of Chemistry, 1977 , vol. 55, p. 548 - 551
1005-62-5
+
106-47-8
对氯苯胺
→
反应条件
4251-65-4
(4-氯苯基)乙醛
反应条件
1: 4-chloro-aniline With hydrogenchloride; sodium nitrite in water 2: 4-methylphenyl vinyl ether With sodium hydrogencarbonate; calcium carbonate; copper dichloride in water; acetone T=25 - 30°C; pH=3 - 4;
参考文献
Naidan; Fesak
Russian Journal of General Chemistry, 2003 , vol. 73, # 9 p. 1419 - 1420
1005-62-5
+
106-40-1
对溴苯胺
→
反应条件
27200-79-9
4-溴苯乙醛
反应条件
1: 4-bromo-aniline With hydrogenchloride; sodium nitrite in water 2: 4-methylphenyl vinyl ether With sodium hydrogencarbonate; calcium carbonate; copper dichloride in water; acetone T=25 - 30°C; pH=3 - 4;
参考文献
Naidan; Fesak
Russian Journal of General Chemistry, 2003 , vol. 73, # 9 p. 1419 - 1420
1005-62-5
+
104-94-9
对甲氧基苯胺
→
反应条件
5703-26-4
4-甲氧基苯乙醛
反应条件
1: 4-methoxy-aniline With hydrogenchloride; sodium nitrite in water 2: 4-methylphenyl vinyl ether With sodium hydrogencarbonate; calcium carbonate; copper dichloride in water; acetone T=25 - 30°C; pH=3 - 4;
参考文献
Naidan; Fesak
Russian Journal of General Chemistry, 2003 , vol. 73, # 9 p. 1419 - 1420
1005-62-5
+
106-49-0
对甲苯胺
→
反应条件
104-09-6
4-甲基苯乙醛
反应条件
1: p-toluidine With hydrogenchloride; sodium nitrite in water 2: 4-methylphenyl vinyl ether With sodium hydrogencarbonate; calcium carbonate; copper dichloride in water; acetone T=25 - 30°C; pH=3 - 4;
参考文献
Naidan; Fesak
Russian Journal of General Chemistry, 2003 , vol. 73, # 9 p. 1419 - 1420
1005-62-5
+
100-01-6
对硝基苯胺
→
反应条件
1460-05-5
反应条件
1: 4-nitro-aniline With hydrogenchloride; sodium nitrite in water 2: 4-methylphenyl vinyl ether With sodium hydrogencarbonate; calcium carbonate; copper dichloride in water; acetone T=25 - 30°C; pH=3 - 4;
参考文献
Naidan; Fesak
Russian Journal of General Chemistry, 2003 , vol. 73, # 9 p. 1419 - 1420
1005-62-5
+
74497-02-2
→
反应条件
122-78-1
反应条件
1: aniline With hydrogenchloride; sodium nitrite in water 2: 4-methylphenyl vinyl ether With sodium hydrogencarbonate; calcium carbonate; copper dichloride in water; acetone T=25 - 30°C; pH=2 - 4; 8 h;
参考文献
Naidan; Fesak
Russian Journal of General Chemistry, 2003 , vol. 73, # 9 p. 1419 - 1420
