1-氯-2-(2-氯乙基)苯合成路线 (共 6 条)
反应条件
1: With methanesulfonyl chloride; triethylamine in toluene T=0°C; 1 h; 2: With lithium chloride in N,N-dimethyl-formamide T=20°C; 24 h;
参考文献
Journal of Organometallic Chemistry, , vol. 663, # 1-2 p. 21 - 31
反应条件
thionyl chloride in tetrahydrofuran 2 h; Heating / reflux;
参考文献
US6342501 B1, ;
Scheme 2 ;
反应条件
1: LiAlH4 / diethyl ether 2: SOCl2, pyridine View Scheme
参考文献
Journal of Organic Chemistry, , vol. 27, p. 3836 - 3843
反应条件
iodine; chlorine in acetic acid
参考文献
Tetrahedron, , vol. 21, p. 245 - 254
参考文献
Bunnett,J.F.; Skorcz,J.A.
Journal of Organic Chemistry, 1962 , vol. 27, p. 3836 - 3843
反应条件
1: aq. ethanol 2: K, liq. NH3 View Scheme
参考文献
Bunnett,J.F.; Skorcz,J.A.
Journal of Organic Chemistry, 1962 , vol. 27, p. 3836 - 3843