2,4,5-三溴-1-甲基-1H-咪唑合成路线 （共 13 条）
反应条件
bromine; sodium acetate in acetic acid 2 h; Ambient temperature;
参考文献
Bahnous, Mebarek; Mouats, Chabane; Fort, Yves; Gros, Philippe C.
Tetrahedron Letters, 2006 , vol. 47, # 12 p. 1949 - 1951
反应条件
n-butyllithium in diethyl ether; hexane T=-70°C; 0.666667 h;
参考文献
Iddon, Brian; Lim, Bee Lan
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 4 p. 735 - 739
反应条件
potassium carbonate in N,N-dimethyl-formamide T=20°C; 14 h;
参考文献
Toguem, Serge-Mitherand Tengho; Langer, Peter
Synlett, 2010 , # 12 p. 1779 - 1782
反应条件
sodium hydride in tetrahydrofuran Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 33, # 40 p. 5865 - 5868
反应条件
chloroform; bromine T=5 - 10°C;
参考文献
Journal of the Chemical Society, , vol. 125, p. 1569
参考文献
Chemische Berichte, , vol. 10, p. 1370
参考文献
Journal of the Chemical Society, , vol. 125, p. 1569
反应条件
ethylmagnesium bromide in tetrahydrofuran T=20°C; 5 h; Inert atmosphere;
参考文献
H. LUNDBECK A/S; KEHLER, Jan; KILBURN, John Paul; NIELSEN, Jacob; PÜSCHL, Ask; LANGGÅRD, Morten; JESSING, Mikkel; MARIGO, Mauro
Patent: WO2013/50527 A1, 2013 ;
Location in patent: Page/Page column 38; 39; 40 ;
反应条件
sodium amalgam; ethanol
参考文献
Wyss
Chemische Berichte, 1877 , vol. 10, p. 1370
参考文献
Wyss
Chemische Berichte, 1877 , vol. 10, p. 1370
