反应条件
1: 2-(5,5-dimetyl-1,3-dioxan-2-yl)-pyrrole With methyl-magnesium iodide in tetrahydrofuran; diethyl ether T=-10 - 20°C; Metallation; 1 h; 2: 2-chloromethyl-1-methanesulfonyl-1H-pyrrole in tetrahydrofuran; diethyl ether T=-10 - 20°C; Alkylation; 2 h; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 63, # 23 p. 8163 - 8169