二(三甲基硅基)碳酰二亚胺合成路线 （共 56 条）
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide HMPTA added to suspn. of CaCN2 in Me3SiCl (stirring); heated to 60°C; heated gradually (120°C, 3 h); cooled; hexane added; ppt. filtered off; dried (vac., 90°C); liquid phase fractionated; elem.anal.;
参考文献
Vostokov, I. A.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 499 - 502
Zhurnal Obshchei Khimii, 1983 , vol. 53, p. 577 - 581
反应条件
ammonium sulfate; mercury(II) oxide reflux 1.) 5 h, 2.) 40 min;
参考文献
Vlasova, N. N.; Pestunovich, A. E.; Voronkov, M. G.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 3 p. 621 - 624,550 - 552
反应条件
triethylamine in dichloromethane Heating;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 745, p. 81 - 86
反应条件
triethylamine in dichloromethane; Petroleum ether Heating;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 745, p. 81 - 86
反应条件
ammonium sulfate 25 h; Heating;
参考文献
Gordetsov, A. S.; Ermolaev, S. A.; Vostokov, I. A.; Skobeleva, S. E.; Trub, E.P.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. 60, # 1.2 p. 139 - 143,122 - 125
反应条件
ammonium sulfate T=135°C; 15 h;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 52, # 4 p. 885 - 890,770 - 774
反应条件
ammonium sulfate T=124 - 147°C; 30 h; Title compound not separated from byproducts;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 52, # 4 p. 885 - 890,770 - 774
反应条件
1.) toluene, RT, 2 h, 2.) toluene, heating, overnight; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 118, # 2 p. 330 - 338
反应条件
in neat (no solvent) isolation from atmosphere; reacting (20°C, 1 - 2 h); distn.;
参考文献
Gordetsov, A. S.; Skobeleva, S. E.; Vostokov, I. A.; Egorochkin, A. N.
Journal of General Chemistry USSR (English Translation), 1980 , vol. 50, p. 515 - 519
Zhurnal Obshchei Khimii, 1980 , vol. 50, p. 632 - 637
参考文献
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, , vol. 31b, p. 1317 - 1321
