(乙氧基乙炔基)(三甲基)硅烷合成路线 （共 15 条）
反应条件
methyllithium 1.) Et2O, hexane, 0 deg C, 30 min, 2.) r.t., overnight; Yield given. Multistep reaction;
参考文献
Mueller, Paul; Pautex, Nicole
Helvetica Chimica Acta, 1991 , vol. 74, # 1 p. 55 - 64
参考文献
Kita, Y.; Akai, S.; Yoshigi, M.; Nakajima, Y.; Yasuda, H.; Tamura, Y.
Tetrahedron Letters, 1984 , vol. 25, # 52 p. 6027 - 6030
反应条件
(i) EtMgBr, (ii) /BRN= 1731135/; Multistep reaction;
参考文献
Shchukovwskaya,L.L.; Pal'chik,R.I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1964 , p. 2129 - 2131
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1964 , p. 2228 - 2230
反应条件
carboxylic acid in dichloromethane further solvent: (CH2)2Cl2;
参考文献
Shchukovskaya,L.L. et al.
Doklady Chemistry, 1965 , vol. 164, p. 887 - 890
Doklady Akademii Nauk SSSR, 1965 , vol. 164, # 2 p. 357 - 360
参考文献
Pelotier, Beatrice; Rajzmann, Michel; Pons, Jean-Marc; Campomanes, Pablo; Lopez, Ramon; Sordo, Tomas L.
European Journal of Organic Chemistry, 2005 , # 12 p. 2599 - 2606
反应条件
methanol 1.) dibutyl ether, 80 deg C, 8 h, 2.) Et2O; Yield given. Multistep reaction;
参考文献
Nikolaeva, S. N.; Zolotareva, A. S.; Ponomarev, S. V.; Petrosyan, V. S.
Russian Chemical Bulletin, 1994 , vol. 43, # 5 p. 857 - 861
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1994 , # 5 p. 911 - 915
反应条件
1: 120 - 130 °C View Scheme
参考文献
Shchukovskaya,L.L. et al.
Doklady Chemistry, 1965 , vol. 164, p. 887 - 890
Doklady Akademii Nauk SSSR, 1965 , vol. 164, # 2 p. 357 - 360
反应条件
mercury(II) diacetate in dichloromethane T=-10°C; 1.5 h;
参考文献
Kita, Yasuyuki; Akai, Shuji; Ajimura, Naomi; Yoshigi, Mayumi; Tsugoshi, Teruhisa; et al.
Journal of Organic Chemistry, 1986 , vol. 51, # 22 p. 4150 - 4158
参考文献
Shchukovskaya,L.L. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1973 , vol. 43, p. 1989 - 1992,1974 - 1976
参考文献
Sakurai,H. et al.
Synthesis, 1979 , p. 740 - 741
