3-甲基-4-硝基苯甲酰胺合成路线 （共 5 条）
反应条件
ammonia in ethylene glycol dimethyl ether; water T=10 - 15°C;
参考文献
WO2008/88927 A1, ;
Page/Page column 26-27 ;
WO 2008/088927 A1
反应条件
phosphorus pentachloride Behandlung des entstandenen Chlorids mit konz. Ammoniak;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 144, p. 182
反应条件
dimethylsulfide borane complex; trifluoroacetic acid in tetrahydrofuran T=60 - 65°C; 2 h;
参考文献
BIOGEN IDEC MA INC.; VERNALIS RESEARCH LIMITED
Patent: WO2008/88927 A1, 2008 ;
Location in patent: Page/Page column 27 ;
WO 2008/088927 A1
反应条件
phosphorus pentachloride
参考文献
Gore,P.H. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1973 , p. 2940 - 2948
参考文献
Roche Palo Alto LLC
Patent: US2007/88015 A1, 2007 ;
Location in patent: Page/Page column 23 ;
