1-苯基-3-三氟甲基吡唑合成路线 (共 12 条)
反应条件
hydroxybenzaldoxime; copper(I) oxide in acetonitrile T=82°C; 24 h;
参考文献
Clapham, Kate M.; Batsanov, Andrei S.; Bryce, Martin R.; Tarbit, Brian
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 10 p. 2155 - 2161
反应条件
hydroxybenzaldoxime; copper(I) oxide in acetonitrile T=82°C; 96 h;
参考文献
Cristau, Henri-Jean; Cellier, Pascal P.; Spindler, Jean-Francis; Taillefer, Marc
European Journal of Organic Chemistry, 2004 , # 4 p. 695 - 709
反应条件
triethylamine in toluene 20 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, p. 3901 - 3904
反应条件
hydrogenchloride in acetonitrile T=20°C; 1 h; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 54, # 31 p. 4076 - 4079
反应条件
sulfuric acid in methanol T=60°C; 24 h; Overall yield = 50 percent; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 53, # 41 p. 5488 - 5491
反应条件
triethylamine in toluene 23 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 6 p. 1841 - 1842
反应条件
1-n-butyl-3-methylimidazolium tetrafluoroborate T=25°C; 1 - 3 h;
参考文献
Catalysis Letters, , vol. 141, # 8 p. 1130 - 1135
反应条件
1: chloroform / 4 h / 20 °C 2: hydrogenchloride / acetonitrile / 1 h / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 31 p. 4076 - 4079
反应条件
1: chloroform / 4 h / 20 °C 2: hydrogenchloride / acetonitrile / 1 h / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 31 p. 4076 - 4079
反应条件
1: chloroform / 4 h / 20 °C 2: hydrogenchloride / acetonitrile / 1 h / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 54, # 31 p. 4076 - 4079