in N,N-dimethyl-formamide
Sonication; glove box under N2; mixed, ultrasonication at 25+/-5°C for 120h; centrifuged, washed (pentane or hexane), extd. (three times with pentane or hexane), evapd., distn.; elem. anal.;
参考文献
Cochran, John C.; Lemieux, Robert P.; Giacobbe, Robert C.; Roitstein, Alexander
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1990 , vol. 20, p. 251 - 262
