反应条件
in tetrachloromethane
Kinetics; byproducts: CO2, CH4, CH3C(O)CH3; further byproducts: CH3CH=CH2,(CH3)3COH, C2Cl6, CHCl3, ClCH=CCl(CH3); open system (argon atmosphere) or evac. sealed ampul; const. temp. (+/-0.1°C) in range 80-85°C; reaction mixt. washing (water), drying (MgSO4), distn. (rectification column); chem. and GLC anal.;
参考文献
Razuvaev, G. A.; Brevnova, T. N.; Chesnokova, T. A.; Troitskaya, L. S.; Shevtsova, M. P.
Journal of General Chemistry USSR (English Translation), 1982 , vol. 52, p. 1624 - 1628
Zhurnal Obshchei Khimii, 1982 , vol. 52, p. 1832 - 1837
