4-碘-2-三氟甲基-1,1,1,2-四氟丁烷合成路线 （共 5 条）
反应条件
ethanolamine; copper(l) chloride T=140°C; P=15001.2 - 18751.5 Torr; 8 h;
参考文献
Arlen; Gauffreteau; Jenneaux; et al.
Bulletin de la Societe Chimique de France, 1985 , vol. NO. 4, p. 562 - 567
反应条件
silver fluoride in diethylene glycol dimethyl ether
1) r.t., 24h, 2) 35 deg C, 72 h;
参考文献
Chen, Li-Fo; Mohtasham, Javid; Gard, Gary L.
Journal of Fluorine Chemistry, 1990 , vol. 48, # 1 p. 107 - 122
反应条件
1: 85 percent / KOH / ethanol / 40 °C
2: 67 percent / 16 h / 195 °C / 30002.4 Torr
3: 75 percent / 10 percent KOH / ethanol / 2 h / Ambient temperature
View Scheme
参考文献
Arlen; Gauffreteau; Jenneaux; et al.
Bulletin de la Societe Chimique de France, 1985 , vol. NO. 4, p. 562 - 567
反应条件
potassium hydroxide in ethanol
T=40°C;
参考文献
Arlen; Gauffreteau; Jenneaux; et al.
Bulletin de la Societe Chimique de France, 1985 , vol. NO. 4, p. 562 - 567
反应条件
1: 85 percent / KOH / ethanol / 40 °C
2: 67 percent / 16 h / 195 °C / 30002.4 Torr
View Scheme
参考文献
Arlen; Gauffreteau; Jenneaux; et al.
Bulletin de la Societe Chimique de France, 1985 , vol. NO. 4, p. 562 - 567
