N,N-二甲基-对苯二胺合成路线 (共 293 条)
反应条件
carbon monoxide; benzene; dodecacarbonyltetrarhodium(0) T=220°C; 6 h;
参考文献
Mise, Takaya; Hong, Pangbu; Yamazaki, Hiroshi
Chemistry Letters, 1980 , p. 439 - 440
反应条件
methoxylamine hydrochloride; n-butyllithium in tetrahydrofuran; hexane T=-78 - 60°C; 24 h; Inert atmosphereCooling with acetone-dry ice; stereospecific reaction;
参考文献
Mlynarski, Scott N.; Karns, Alexander S.; Morken, James P.
Journal of the American Chemical Society, 2012 , vol. 134, # 40 p. 16449 - 16451,3
反应条件
1: With trifluoromethyl amino ketone; potassium carbonate; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in 1,4-dioxane T=75°C; 2: With methanol in 1,4-dioxane T=75°C; Further stages.;
参考文献
Tao, Chuan-Zhou; Li, Juan; Fu, Yao; Liu, Lei; Guo, Qing-Xiang
Tetrahedron Letters, 2008 , vol. 49, # 1 p. 70 - 75
反应条件
1: With hydrazine hydrate T=135°C; 3 h; 2: With potassium hydroxide T=135°C; 24 h;
参考文献
Diez-Cecilia, Elena; Kelly, Brendan; Rozas, Isabel
Tetrahedron Letters, 2011 , vol. 52, # 50 p. 6702 - 6704
反应条件
methanol; hydrogen T=99.84°C; P=9750.98 Torr; 1.63333 h; Autoclave;
参考文献
Catalysis Communications, , vol. 41, p. 115 - 118
反应条件
diethylamine in cyclohexane Ambient temperatureIrradiation;
参考文献
Journal of the American Chemical Society, , vol. 110, # 24 p. 8092 - 8098
反应条件
water T=100°C; 8 h; Inert atmosphere;
参考文献
Wang, Jia; Liang, Yan-Liang; Qu, Jin
Chemical Communications, 2009 , # 34 p. 5144 - 5146
反应条件
formic acid; zinc in methanol T=20°C; 0.216667 h;
参考文献
Tetrahedron Letters, , vol. 43, # 7 p. 1329 - 1331
反应条件
ammonium formate; nickel in methanol T=20°C; 0.133333 h;
参考文献
Prasad; Gowda, Shankare; Gowda, D. Channe
Synthetic Communications, 2004 , vol. 34, # 1 p. 1 - 10
反应条件
formic acid; zinc in methanol T=20°C; 0.133333 h;
参考文献
Tetrahedron Letters, , vol. 43, # 7 p. 1329 - 1331