3,4-二羟基-2'-氯苯乙酮合成路线 (共 71 条)
反应条件
1: 96 percent / 2,6-Lutidine / tetrahydrofuran / 1 h / 0 °C
2: 96 percent / BH3 / CBS catalyst R-oxazaborolidine (8) / tetrahydrofuran / 0.08 h
3: 92 percent / NaI / acetone / 72 h / Heating
4: 95 percent / Imidazole / dimethylformamide / 0.08 h / 23 °C
5: 88 percent / 6.5 h / 80 °C
6: 81 percent / KF, HCl / methanol / 2.5 h / 23 °C
View Scheme
参考文献
Corey; Link, John O.
Tetrahedron Letters, 1990 , vol. 31, # 5 p. 601 - 604