反应条件
1.1: anhydrous tetramethylammonium chloride; trichlorophosphate / 16 h / 130 °C 1.3: pH 7 - 8 2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / toluene; 1,4-dioxane / 18 h / 75 °C / Inert atmosphere 3.1: ammonia / methanol / 20 h / 60 °C 4.1: trifluoroacetic anhydride; pyridine / dichloromethane / 24 h / 0 °C View Scheme
参考文献
Bolli, Martin; Lescop, Gyrille; Mathys, Boris; Mueller, Claus; Nayler, Oliver; Steiner, Beat
Patent: US2011/46170 A1, 2011 ;