2-[(R)-甲基亚磺酰]-1H-苯并咪唑合成路线 （共 8 条）
反应条件
2,4,6-trichloro-1,3,5-triazine; potassium iodide in acetonitrile T=20°C; 0.25 h; chemoselective reaction;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad M.; Sohrabnezhad, Samira
Tetrahedron Letters, 2011 , vol. 52, # 48 p. 6420 - 6423
参考文献
Graber, David R.; Morge, Raymond A.; Sih, John C.
Journal of Organic Chemistry, 1987 , vol. 52, # 20 p. 4620 - 4622
反应条件
1: aq. ethanol / 25 °C
2: m-chloroperbenzoic acid / CHCl3 / 0.17 h / 0 - 5 °C
3: aq. ethanol / 25 °C
View Scheme
参考文献
Graber, David R.; Morge, Raymond A.; Sih, John C.
Journal of Organic Chemistry, 1987 , vol. 52, # 20 p. 4620 - 4622
反应条件
1: aq. ethanol / 25 °C
2: m-chloroperbenzoic acid / CHCl3 / 0.17 h / 0 - 5 °C
3: aq. ethanol / 25 °C
4: m-chloroperbenzoic acid / CHCl3 / 0.17 h / 0 - 5 °C
5: aq. ethanol / 15 h / 75 °C
View Scheme
参考文献
Graber, David R.; Morge, Raymond A.; Sih, John C.
Journal of Organic Chemistry, 1987 , vol. 52, # 20 p. 4620 - 4622
反应条件
in ethanol
1 h; Heating;
参考文献
Hirai, K; Koike, H; Ishiba, T; Ueda, S; Makino, I; et al.
European Journal of Medicinal Chemistry, 1991 , vol. 26, # 2 p. 143 - 158
反应条件
1: 2,4,6-trichloro-1,3,5-triazine; potassium iodide / acetonitrile / 0.25 h / 20 °C
2: 2,4,6-trichloro-1,3,5-triazine; dihydrogen peroxide / water; acetonitrile / 0.33 h / 20 °C
View Scheme
参考文献
Bahrami, Kiumars; Khodaei, Mohammad M.; Sohrabnezhad, Samira
Tetrahedron Letters, 2011 , vol. 52, # 48 p. 6420 - 6423
参考文献
Graber, David R.; Morge, Raymond A.; Sih, John C.
Journal of Organic Chemistry, 1987 , vol. 52, # 20 p. 4620 - 4622
反应条件
1: aq. ethanol / 25 °C
2: m-chloroperbenzoic acid / CHCl3 / 0.17 h / 0 - 5 °C
3: aq. ethanol / 25 °C
View Scheme
参考文献
Graber, David R.; Morge, Raymond A.; Sih, John C.
Journal of Organic Chemistry, 1987 , vol. 52, # 20 p. 4620 - 4622
