(R)-(2-氧代-3-氧杂环丁基)氨基甲酸苄酯合成路线 （共 6 条）
反应条件
MeO2CN=NCO2Me; triphenylphosphine in tetrahydrofuran T=20°C; 2.5 h;
参考文献
Arnold; Kalantar; Vederas
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 7105 - 7109
反应条件
triphenylphosphine; diethylazodicarboxylate in acetonitrile T=-35 - 5°C; 12 h;
参考文献
AVENTIS PHARMA DEUTSCHLAND GMBH
Patent: WO2004/22553 A1, 2004 ;
Location in patent: Page/Page column 12-13 ;
WO 2004/022553 A1
反应条件
1: 82 percent / sodium bicarbonate / H2O; tetrahydrofuran / 1.5 h / 20 °C 2: 40 percent / dimethyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 3.33 h / -78 - 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 67, # 5 p. 1536 - 1547
反应条件
ammonia in tetrahydrofuran T=0°C; 1 h;
参考文献
Arnold; Kalantar; Vederas
Journal of the American Chemical Society, 1985 , vol. 107, # 24 p. 7105 - 7109
反应条件
in tetrahydrofuran; methanol T=22°C; 0.416667 h;
参考文献
Journal of the American Chemical Society, , vol. 107, # 24 p. 7105 - 7109
反应条件
in tetrahydrofuran; methanol T=22°C; 0.416667 h;
参考文献
Journal of the American Chemical Society, , vol. 107, # 24 p. 7105 - 7109
