1-(4-溴苯甲酰基)哌啶合成路线 （共 12 条）
反应条件
4-bromooctafluorobutanetriethoxysilane; zinc diacetate in tetrahydrofuran T=40°C; Inert atmosphere;
参考文献
Das, Shoubhik; Addis, Daniele; Zhou, Shaolin; Junge, Kathrin; Beller, Matthias
Journal of the American Chemical Society, 2010 , vol. 132, # 6 p. 1770 - 1771
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in trichloroethane, 1,1,2-; water
T=90°C; 12 h;
参考文献
Li, Huamin; Xie, Jin; Xue, Qicai; Cheng, Yixiang; Zhu, Chengjian
Tetrahedron Letters, 2012 , vol. 53, # 48 p. 6479 - 6482,4
反应条件
triethylamine in dichloromethane
T=20°C; Inert atmosphere;
参考文献
Das, Shoubhik; Addis, Daniele; Zhou, Shaolin; Junge, Kathrin; Beller, Matthias
Journal of the American Chemical Society, 2010 , vol. 132, # 6 p. 1770 - 1771
反应条件
tert.-butylhydroperoxide; potassium carbonate in tetrahydrofuran
T=80°C; 12 h; Sealed tube;
参考文献
Zhao, Qiong; Li, Hongji; Wang, Lei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 39 p. 6772 - 6779
反应条件
dihydrogen peroxide
T=70°C; 2.5 h; Reflux; Catalytic behavior;
参考文献
Sharma; Sharma, Shivani
Dalton Transactions, 2014 , vol. 43, # 3 p. 1292 - 1304
反应条件
tert.-butylhydroperoxide; potassium carbonate in tetrahydrofuran
T=80°C; 12 h; Sealed tube;
参考文献
Zhao, Qiong; Li, Hongji; Wang, Lei
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 39 p. 6772 - 6779
参考文献
Takahata, Hiroki; Yamazaki, Takao; Aoe, Keiichi
Journal of Organic Chemistry, 1985 , vol. 50, # 23 p. 4648 - 4650
反应条件
tert.-butylhydroperoxide; FeCl3·6H2O in water; acetonitrile
T=85°C; Inert atmosphere;
参考文献
Gaspa, Silvia; Porcheddu, Andrea; De Luca, Lidia
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3803 - 3807
反应条件
1: 17 percent / Et3N / CH2Cl2 / 4 h / Ambient temperature
2: 88 percent / 3 h / 160 °C
View Scheme
参考文献
Takahata, Hiroki; Yamazaki, Takao; Aoe, Keiichi
Journal of Organic Chemistry, 1985 , vol. 50, # 23 p. 4648 - 4650
反应条件
1: N-chloro-succinimide / acetonitrile / 20 °C / |Inert atmosphere
2: tert.-butylhydroperoxide; FeCl3·6H2O / acetonitrile; water / 85 °C / |Inert atmosphere
View Scheme
参考文献
Gaspa, Silvia; Porcheddu, Andrea; De Luca, Lidia
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3803 - 3807
