3-(2,4-二氯苯基)-丙醛合成路线 （共 4 条）
反应条件
tetrabutyl-ammonium chloride; palladium diacetate; sodium hydrogencarbonate T=80°C; 30 h;
参考文献
Gangjee, Aleem; Qiu, Yibin; Kisliuk, Roy L.
Journal of Heterocyclic Chemistry, 2004 , vol. 41, # 6 p. 941 - 946
反应条件
1: With diisobutylaluminium hydride in hexanes; dichloromethane T=-78°C; 2 h; 2: With water; sodium hydrogencarbonate in hexanes; dichloromethane T=20°C;
参考文献
WO2008/99019 A1, ;
Page/Page column 53 ;
反应条件
pyridinium chlorochromate in dichloromethane T=0°C; 4 h;
参考文献
Houjeiry, Tania I.; Poe, Sarah L.; McQuade, D. Tyler
Organic Letters, 2012 , vol. 14, # 17 p. 4394 - 4397
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / 80 °C / |Cooling with ice; |Inert atmosphere 2: pyridinium chlorochromate / dichloromethane / 4 h / 0 °C View Scheme
参考文献
Organic Letters, , vol. 14, # 17 p. 4394 - 4397
