1,3,5-O-次甲基-myo-纤维醇合成路线 （共 11 条）
反应条件
Amberlyst 15 in N,N-dimethyl-formamide T=100°C; 3 h;
参考文献
Krief, Alain; Dumont, Willy; Billen, Denis; Letesson, Jean-Jacques; Lestrate, Pascal; Murphy, Peter J.; Lacroix, Damien
Tetrahedron Letters, 2004 , vol. 45, # 7 p. 1461 - 1463
反应条件
TSA in N,N-dimethyl-formamide T=110°C; 5 h;
参考文献
Ahn, Young-Hoon; Chang, Young-Tae
Chemistry - A European Journal, 2004 , vol. 10, # 14 p. 3543 - 3547
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide T=100°C; 22 h; Inert atmosphere;
参考文献
Peng, Jianbiao; Kishi, Yoshito
Organic Letters, 2012 , vol. 14, # 1 p. 86 - 89
反应条件
sodium methylate in methanol Deacetylation;
参考文献
Carbohydrate Research, , vol. 325, # 4 p. 313 - 320
反应条件
1: 1.) vinyl acetate, lipoprotein lipase from Pseudomonas, 2.) pyridine, DMAP, 3.) HCl/MeOH 2: 80 percent / acetone / 96 h / 35 °C / lipoprotein lipase from Pseudomonas sp. View Scheme
参考文献
Andersch, P.; Schneider, M. P.
Tetrahedron: Asymmetry, 1993 , vol. 4, # 10 p. 2135 - 2138
反应条件
sodium hydride in N,N-dimethyl-formamide 0 deg C, 2 h to RT, 18 h;
参考文献
Schmitt, Laurent; Spiess, Bernard; Schlewer, Gilbert
Tetrahedron Letters, 1998 , vol. 39, # 27 p. 4817 - 4820
反应条件
sodium hydride in N,N-dimethyl-formamide
参考文献
Wessig, Pablo; Moellnitz, Kristian; Huebner, Sebastian
Synlett, 2010 , # 10 p. 1497 - 1500
反应条件
1: 1) NaH / 1) DMF 2: 1) NaH / 1) DMF View Scheme
参考文献
Billington, David C.; Baker, Raymond; Kulagowski, Janusz J.; Mawer, Ian M.; Vacca, Joseph P.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1423 - 1429
反应条件
1H-imidazole; sodium hydride 1) DMF, r.t., 1 h, 2) DMF, 1 h; Yield given. Multistep reaction;
参考文献
Billington, David C.; Baker, Raymond; Kulagowski, Janusz J.; Mawer, Ian M.; Vacca, Joseph P.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 1423 - 1429
反应条件
1: NaH / dimethylformamide / 20 °C
2: HCl / methanol / 1 h / Heating
View Scheme
参考文献
Yuan, Chengye; Zhai, Haixiao; Li, Yubao; Wang, Sanshan
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 69, # 1-2 p. 71 - 74
