1,1'-carbonyldiimidazole in tetrahydrofuran Ambient temperature;

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in tetrahydrofuran; water

1: KOH / propan-2-ol / 55 - 60 °C 2: 69 percent / pyridinium chlorochromate / CH2Cl2 3: 99 percent / NH2OH*HCl, NaOH / H2O; ethanol / 0.17 h / Heating 4: 93 percent / N,N'-carbonyldiimidazole / tetrahydrofuran / Ambient temperature View Scheme

1: 99 percent / NH2OH*HCl, NaOH / H2O; ethanol / 0.17 h / Heating 2: 93 percent / N,N'-carbonyldiimidazole / tetrahydrofuran / Ambient temperature View Scheme

1: 69 percent / pyridinium chlorochromate / CH2Cl2 2: 99 percent / NH2OH*HCl, NaOH / H2O; ethanol / 0.17 h / Heating 3: 93 percent / N,N'-carbonyldiimidazole / tetrahydrofuran / Ambient temperature View Scheme

1: NaBH4 / propan-2-ol 2: KOH / propan-2-ol / 55 - 60 °C 3: 69 percent / pyridinium chlorochromate / CH2Cl2 4: 99 percent / NH2OH*HCl, NaOH / H2O; ethanol / 0.17 h / Heating 5: 93 percent / N,N'-carbonyldiimidazole / tetrahydrofuran / Ambient temperature View Scheme