4-氟-5-甲基苯-1,2-二胺合成路线 （共 6 条）
反应条件
hydrogen; nickel in ethanol Ambient temperature;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 39, # 3 p. 213 - 218
反应条件
1: 15.8 g / 0.83 h 2: 66 percent / HNO3 / 0.25 h 3: 97 percent / 86percent KOH / H2O; methanol / 0.5 h / 60 °C 4: 93 percent / H2 / Raney nickel / ethanol / Ambient temperature View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 39, # 3 p. 213 - 218
反应条件
1: 66 percent / HNO3 / 0.25 h 2: 97 percent / 86percent KOH / H2O; methanol / 0.5 h / 60 °C 3: 93 percent / H2 / Raney nickel / ethanol / Ambient temperature View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 39, # 3 p. 213 - 218
反应条件
1: 97 percent / 86percent KOH / H2O; methanol / 0.5 h / 60 °C 2: 93 percent / H2 / Raney nickel / ethanol / Ambient temperature View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 39, # 3 p. 213 - 218
反应条件
1: H2 / Raney nickel / ethanol / Ambient temperature 2: 15.8 g / 0.83 h 3: 66 percent / HNO3 / 0.25 h 4: 97 percent / 86percent KOH / H2O; methanol / 0.5 h / 60 °C 5: 93 percent / H2 / Raney nickel / ethanol / Ambient temperature View Scheme
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 39, # 3 p. 213 - 218
反应条件
2: 1.) H2, 3.) NH4OH / 1.) Raney nickel / 1.) EtOH, RT, 25 min, 2.) 3.5 h, 3.) H2O
View Scheme
参考文献
Grivas, Spiros
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1985 , vol. 39, # 3 p. 213 - 218
