2-甲基-2-丙基N2,N6-二{[(2-甲基-2-丙基)氧基]羰基}-6-氧代-L-赖氨酸酯合成路线 （共 5 条）
反应条件
1: 82 percent / TFA / 0.17 h / Ambient temperature 2: 83 percent / HCl (6N) / H2O / 5 h / Heating View Scheme
参考文献
Yoshifuji, Shigeyuki; Tanaka, Ken-ichi; Nitta, Yoshihiro
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 7 p. 2994 - 3001
反应条件
ruthenium(IV) oxide; sodium periodate in ethyl acetate
6 h; Ambient temperature;
参考文献
Yoshifuji, Shigeyuki; Tanaka, Ken-ichi; Nitta, Yoshihiro
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 7 p. 2994 - 3001
反应条件
ruthenium(IV) oxide; Sodium bromate in water; ethyl acetate
5.5 h, 45 deg C, then 18 h, RT;
参考文献
Nevill Jr., C. Richard; Angell, Paul T.
Tetrahedron Letters, 1998 , vol. 39, # 32 p. 5671 - 5674
反应条件
1: 1.) NaOH, 2.) BF3*Et2O / 1.) dioxane, H2O, 2.) c-hexane, CH2Cl2
2: 86 percent / NaBrO3, RuO2 / ethyl acetate; H2O / 5.5 h, 45 deg C, then 18 h, RT
View Scheme
参考文献
Nevill Jr., C. Richard; Angell, Paul T.
Tetrahedron Letters, 1998 , vol. 39, # 32 p. 5671 - 5674
反应条件
trifluoroacetic acid
0.166667 h; Ambient temperature;
参考文献
Yoshifuji, Shigeyuki; Tanaka, Ken-ichi; Nitta, Yoshihiro
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 7 p. 2994 - 3001
