Kostiner,E. et al.
Journal of Organometallic Chemistry, 1968 , vol. 15, p. 383 - 395
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Reddy et al.
Nature (London, United Kingdom), 1968 , vol. 217, p. 740
in tetrahydrofuran
byproducts: YbCl2; HgCl2 was added under N2 to soln. of Yb-complex in THF at -78°C for 0.5 h, solvent was removed under vac., H2O was added, residue was hydrolysed with ether/H2O or CHCl3/H2O; organic layer was washed with aq. NaHCO3, dried, evapd., recrystd. from aq. MeOH and petrol;
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Deacon, Glen B.; Mackinnon, Peter I.; Tuong, Tran D.
Australian Journal of Chemistry, 1983 , vol. 36, p. 43 - 54
(C6F5)Hg(OCOCF3) in not given
heating in a sealed ampule for 46 h at 240°C; filtn., distn.;
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Bardin, V. V.; Aparina, L. N.; Furin, G. G.
Journal of General Chemistry USSR (English Translation), 1991 , vol. 61, p. 1291 - 1294
Zhurnal Obshchei Khimii, 1991 , vol. 61, p. 1414 - 1417
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反应条件
n-BuLi in tetrahydrofuran
to Cs(HCB11F11) in THF n-BuLi in hexane was added at 0°C, warmed to room temp., stirred for 1 h, soln. C6F5HgCl in THF was added at o or -78°C;
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Himmelspach, Alexander; Sprenger, Jan A. P.; Warneke, Jonas; Zaehres, Manfred; Finze, Maik
Organometallics, 2012 , vol. 31, # 4 p. 1566 - 1577
