in neat (no solvent) heating in a closed tube at 260°C, 9 days;;
参考文献
Burdon, J.; Coe, P. L.; Fulton, M.
Journal of the Chemical Society, 1965 , p. 2094 - 2096
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Gmelin Handbook: F: PerFHalOrg.4, 4.3.1, page 181 - 183
in tetrahydrofuran byproducts: THF; under N2, reaction time: 72 h;
参考文献
Deacon, G. B.; Forsyth, C. M.
Inorganica Chimica Acta, 1988 , vol. 154, p. 121 - 122
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反应条件
in tetrahydrofuran stirring mercury compound and Yb in THF under N2 at room temp. for 4 h, filtn., addn. of degassed phenylacetylene; addn. of light petroleum, cooling, elem. anal., IR;
参考文献
Deacon, Glen B.; Koplick, Andrew J.; Tuong, Tran D.
Australian Journal of Chemistry, 1982 , vol. 35, p. 941 - 950
