反应条件
pyridine; water in tetrahydrofuran; diethyl ether to Sn compd. in THF added BH3 (B/Sn ratio 1/1) under N2 at room temp., stirred for 1 h, refluxed for 1h, cooled to room temp., added H2O, stirred for 30 min at room temp, extd. with Et2O, dried (MgSO4), heated with pentane, evapd., added Et2O and C5H5N;
参考文献
Pickles, G. M.; Spencer, T.; Thorpe, F. G.; Chopa, A. B.; Podesta, J. C.
Journal of Organometallic Chemistry, 1984 , vol. 260, # 1 p. 7 - 16
