1: With n-butyllithium; zirconocene dichloride in tetrahydrofuran; hexane T=-78 - 20°C; 2: With CuCl*2LiCl in tetrahydrofuran; hexane T=45°C; 1 h; 3: With N-bromosuccinmide in tetrahydrofuran; hexane Further stages.;
参考文献
Chinkov, Nicka; Majumdar, Swapan; Marek, Ilan
Journal of the American Chemical Society, 2002 , vol. 124, # 35 p. 10282 - 10283
1: With (1-butene)ZrCp2 in tetrahydrofuran T=20°C; 2: With copper(l) chloride; lithium chloride in tetrahydrofuran 3: With hydrogenchloride in tetrahydrofuran
1: With dibutylzirconocene in tetrahydrofuran; hexane T=-78 - 20°C; 2: With hydrogenchloride in tetrahydrofuran; hexane T=20°C; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 125, # 43 p. 13258 - 13264