2,4,4-三氯-3-(二氯甲基)巴豆酸甲酯合成路线 (共 3 条)
反应条件
formic acid; sulfuric acid; water T=120°C; Yield given;
参考文献
Padmapriya, Abeysinghe A.; Just, George; Lewis, Norman G.
Canadian Journal of Chemistry, 1985 , vol. 63, p. 828 - 832
反应条件
triethylamine in diethyl ether
0.5 h; Ambient temperature;
参考文献
Padmapriya, Abeysinghe A.; Just, George; Lewis, Norman G.
Canadian Journal of Chemistry, 1985 , vol. 63, p. 828 - 832
反应条件
1: 100 percent / ferric chloride, chlorine / CH2Cl2 / 14 h / Ambient temperature
2: 80 percent / triethylamine / diethyl ether / 0.5 h / Ambient temperature
View Scheme
参考文献
Padmapriya, Abeysinghe A.; Just, George; Lewis, Norman G.
Canadian Journal of Chemistry, 1985 , vol. 63, p. 828 - 832