反应条件
Multi-step reaction with 6 steps 1: 97 percent / 4 h / 160 °C2: acetyl chloride / 16 h / Heating3: 80 percent / lithium aluminum hydride / diethyl ether / 3.5 h / Heating4: 98 percent / thionyl chloride / CHCl3 / 2 h / Heating5: 60 percent / tricaprylmethylammonium chloride / H2O / 48 h / 100 °C6: 42 percent / conc. hydrochloric acid / 5 h / Heating
参考文献
Nielsen, Lone; Brehm, Lotte; Krogsgaard-Larsen, Povl Journal of Medicinal Chemistry, 1990 , vol. 33, # 1 p. 71 - 77
