(S)-1-苯基-1,3-丙二醇合成路线 （共 41 条）
反应条件
sodium tetrahydroborate in methanol Yield given;
参考文献
Tetrahedron Letters, , vol. 37, # 51 p. 9253 - 9254
反应条件
1: 64 percent / H2O / 48 h / 27 °C / Geotrichium candidum 2: 80 percent / LiAlH4 / diethyl ether / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 48, # 33 p. 6769 - 6776
反应条件
potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate in tetrahydrofuran; methanol 18 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 114, # 6 p. 2121 - 2128
反应条件
potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate in tetrahydrofuran; methanol 18 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 114, # 6 p. 2121 - 2128
反应条件
potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate in tetrahydrofuran; methanol 18 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 114, # 6 p. 2121 - 2128
反应条件
1: aq. PPTS / acetone 2: 1.) (R,R)-ethylenebis(tetrahydroindenyl) titanium difluoride, PhSiH3, pyrrolidine, MeOH, polymethylhydrosiloxane, 2.) MeOH / 1.) THF, RT, 2.) THF, 15 deg C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 121, # 24 p. 5640 - 5644
反应条件
1: LiAlH4 2: aq. PPTS / acetone 3: 1.) (R,R)-ethylenebis(tetrahydroindenyl) titanium difluoride, PhSiH3, pyrrolidine, MeOH, polymethylhydrosiloxane, 2.) MeOH / 1.) THF, RT, 2.) THF, 15 deg C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 121, # 24 p. 5640 - 5644
反应条件
1: With tetrachlorosilane; N-ethyl-N,N-diisopropylamine in dichloromethane T=-72°C; 1 h; 2: With oxygen; ozone in dichloromethane T=-78°C; 0.333333 h; 3: With lithium aluminium tetrahydride in tetrahydrofuran; dichloromethane T=65°C; 1.5 h; Further stages. Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 72, # 15 p. 5668 - 5688
反应条件
1: With oxygen; ozone in dichloromethane T=-78 - 20°C; 2 h; 2: With lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 1 h;
参考文献
Chen, Jack L.-Y.; Scott, Helen K.; Hesse, Matthew J.; Willis, Christine L.; Aggarwal, Varinder K.
Journal of the American Chemical Society, 2013 , vol. 135, # 14 p. 5316 - 5319
反应条件
sodium hydroxide; borane-THF 1) THF, 0 deg C to RT, 1 h, 2) 60 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 57, # 15 p. 4289 - 4292
