叔丁基3-溴甲基-吲哚-1-羧酸酯合成路线 (共 11 条)
反应条件
in tetrachloromethane; hexane
参考文献
Indiana University Foundation
Patent: US5554753 A1, 1996 ;
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 2 h; Heating;
参考文献
Zhao, Shuo; Gan, Tong; Yu, Peng; Cook, James M.
Tetrahedron Letters, 1998 , vol. 39, # 39 p. 7009 - 7012
反应条件
1: 99 percent / DMAP / acetonitrile / Ambient temperature 2: 95 percent / NBS, AIBN / CCl4 / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 39, # 39 p. 7009 - 7012
反应条件
1: 99 percent / DMAP / acetonitrile / Ambient temperature 2: 95 percent / NBS, AIBN / CCl4 / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 39, # 39 p. 7009 - 7012
反应条件
1: 92 percent / sodium borohydride / ethanol / 6 h 2: 83 percent / Br2; Ph3P; Et3N / CCl4 / 72 h / 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 30, # 12 p. 2143 - 2159
反应条件
1: 1 N KOH / tetrahydrofuran; H2O / 6 h / Ambient temperature 2: 100 percent / NaBH4 / ethanol / 6 h / 20 °C 3: triphenylphosphane, Br2 / CCl4 / 72 h / Ambient temperature View Scheme
参考文献
Liebigs Annalen der Chemie, , # 2 p. 413 - 417
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile Yield given;
参考文献
Tetrahedron Letters, , vol. 36, # 50 p. 9133 - 9136
反应条件
1: 1 N KOH / tetrahydrofuran; H2O / 6 h / Ambient temperature 2: 100 percent / NaBH4 / ethanol / 6 h / 20 °C 3: triphenylphosphane, Br2 / CCl4 / 72 h / Ambient temperature View Scheme
参考文献
Liebigs Annalen der Chemie, , # 2 p. 413 - 417
反应条件
Yield given. Multistep reaction;
参考文献
Alonso, Francisco; Davies, Stephen G.; Elend, Almut S.; Haggitt, Jane L.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 2 p. 257 - 264
参考文献
Alonso, Francisco; Davies, Stephen G.; Elend, Almut S.; Haggitt, Jane L.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 2 p. 257 - 264