4-氧-4,5,6,7-四氢-1氢-吲哚-3-甲酸乙酯合成路线 （共 4 条）
反应条件
1: 82 percent / NaBH4 / ethanol / 4 h / 40 °C 2: 80 percent / p-toluenesulfonic acid / 10percent Pd/C / dioxane / 8 h / 100 °C View Scheme
参考文献
Croce, Piero Dalla; Rosa, Concetta La
Synthesis, 1984 , # 11 p. 982 - 983
反应条件
hydrazine monohydrochloride; triethylamine in methanol; N,N-dimethyl-formamide
参考文献
Merck Sharp and Dohme Ltd.
Patent: US6395905 B1, 2002 ;
US 6395905 B1
反应条件
hydrazine in ethanol
4 h; Ambient temperature;
参考文献
Croce, Piero Dalla; Rosa, Concetta La
Synthesis, 1984 , # 11 p. 982 - 983
反应条件
1: 52 percent / ZnCl2 / CH2Cl2; diethyl ether / 1 h / 0 °C
2: 72 percent / NH2-NH2 / ethanol / 4 h / Ambient temperature
View Scheme
参考文献
Croce, Piero Dalla; Rosa, Concetta La
Synthesis, 1984 , # 11 p. 982 - 983
