triethylamine in tetrahydrofuran
byproducts: Et3N*HCl; dropwise addn. of Ge compd. soln. to soln. of MeP(O)(OH)2 and triethylamine with stirring; filtration; addn. of oxirane; stirring,2h; all under inert gas; detn. by NMR;
参考文献
Barrau, J.; Rima, G.; Satge, J.
Phosphorus, Sulfur, and Silicon and the Related Elements, 1990 , vol. 54, p. 23 - 30
triethylamine in benzene
byproducts: (C2H5)3NHCl; addn. of NEt3 to the Ge compounds in benzene (inert gas) and heating at 70°C for 4 days in a sealed ampoule; filtn.;
参考文献
Riviere-Baudet, Monique; Morere, Alain; Onyszchuk, Mario; Satge, Jacques
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 70, # 1/2 p. 75 - 90
