反应条件
1: 64 percent / NaOAc, pyridinium chlorochromate / CH2Cl2 / 1 h / Ambient temperature
2: 1.) KOC(CH3)3 / 1.) THF, 0 deg C, 10 min, 2.) 0 deg C, 3.75 h
3: 88percent HCO2H / tetrahydrofuran / 20 h / 0 °C
View Scheme
参考文献
Porter, N. A.; Ziegler, C. B.; Khouri, F. F.; Roberts, D. H.
Journal of Organic Chemistry, 1985 , vol. 50, # 13 p. 2252 - 2258
