2-氟-2-丙烯酸 2,2,3,3-四氟丙基酯合成路线 （共 3 条）
参考文献
Boguslavskaya, L. S.; Chuvatkin, N. N.
Journal of Fluorine Chemistry, 1991 , vol. 54, # 1-3 p. 138
反应条件
1: 85 percent / bromine trifluoride, 1 mol percent tin tetrachloride / 1,1,2-trichloro-1,2,2-trifluoro-ethane / 2.5 h / 20 - 30 °C
2: 90 percent / triethylamine / CH2Cl2 / 20 - 40 °C
View Scheme
参考文献
Kartashov, A. V.; Chuvatkin, N. N.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 12.1 p. 2243 - 2248
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 12 p. 2522 - 2528
反应条件
1: bromine trichloride, 1 percent pyridine / neat (no solvent)
2: 85 percent / bromine trifluoride, 1 mol percent tin tetrachloride / 1,1,2-trichloro-1,2,2-trifluoro-ethane / 2.5 h / 20 - 30 °C
3: 90 percent / triethylamine / CH2Cl2 / 20 - 40 °C
View Scheme
参考文献
Kartashov, A. V.; Chuvatkin, N. N.; Boguslavskaya, L. S.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 12.1 p. 2243 - 2248
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 12 p. 2522 - 2528
