[1,2-双(二环己基膦)乙烷]氯化钯(II)合成路线 （共 2 条）
反应条件
in dichloromethane
(N2); addn. of CH2Cl2 soln. of palladium compd. to CH2Cl2 soln. of phosphine deriv., stirring at room temp. for 4 h; evapn., washing with pentane, drying in vac. for 1 d;
参考文献
Arumugam, Kuppuswamy; Shaw, Mohamed C.; Chandrasekaran; Villagran, Dino; Gray, Thomas G.; Maguey, Joel T.; Donahue, James P.
Inorganic Chemistry, 2009 , vol. 48, # 22 p. 10591 - 10607
反应条件
in benzene
mixt. stirred for 2 h; addn. of pentane, solid filtered off, washed with pentane, and dried under vac.; elem. anal.;
参考文献
Diversi, Pietro; Ingrosso, Giovanni; Lucherini, Antonio; Lumini, Tito; Marchetti, Fabio; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 133 - 140
