1: para-bromotoluene With n-butyllithium in tetrahydrofuran
T=-70°C; 0.5 h;
2: DMTBN in tetrahydrofuran
T=-60 - 10°C; 1 h;
参考文献
Nenajdenko, V. G.; Druzhinin, S. V.; Balenkova, E. S.
Russian Chemical Bulletin, 2004 , vol. 53, # 2 p. 435 - 442
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 2004 , # 2 p. 416 - 422
Gazit, Aviv; Rappoport, Zvi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 12 p. 2863 - 2870
piperidine; acetic acid in benzene
170 h; Heating; Title compound not separated from byproducts;
参考文献
Gazit, Aviv; Rappoport, Zvi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 12 p. 2863 - 2870