2-(N,N-二异丙氨基)氯乙烷合成路线 （共 19 条）
参考文献
Maillard,J. et al.
Chimica Therapeutica, 1970 , vol. 5, p. 1 - 9
反应条件
lithium 1.) THF, 2.) THF, 0 deg C, 12 h; Yield given. Multistep reaction;
参考文献
Azzena; Melloni; Fenude; Fina; Marchetti; Sechi
Synthetic Communications, 1994 , vol. 24, # 5 p. 591 - 599
反应条件
(i) NaH, DMF, (ii) /BRN= 605346/; Multistep reaction;
参考文献
US Vitamins
Patent: DE2036181 , 1971 ;
Chem.Abstr., 1971 , vol. 74, # 99671
反应条件
(i) NaH, DMF, (ii) /BRN= 605346/; Multistep reaction;
参考文献
US Vitamins
Patent: DE2036181 , 1971 ;
Chem.Abstr., 1971 , vol. 74, # 99671
反应条件
(i) NaH, DMF, (ii) /BRN= 605346/; Multistep reaction;
参考文献
US Vitamins
Patent: DE2036181 , 1971 ;
Chem.Abstr., 1971 , vol. 74, # 99671
反应条件
1: (2-methoxy-5-methylphenyl)phenylmethane; 3-benzyl-4-methylanisole With n-butyllithium in tetrahydrofuran T=-78 - 0°C; 6 h; 2: 1-diisopropylamino-2-chloroethane in tetrahydrofuran T=-78 - 20°C; 2 h; Product distribution / selectivity;
参考文献
US7268257 B1, ;
Page/Page column 9; 9-10 ;
反应条件
1: KOH 2: LiNH2, NH3 View Scheme
参考文献
Moskowitz,H. et al.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1967 , vol. 264, p. 1406 - 1408
参考文献
Cusic; Robinson
Journal of Organic Chemistry, 1951 , vol. 16, p. 1921,1928
反应条件
thionyl chloride; benzene
参考文献
Wright et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 3536,3537
Full Text Show Details
Vecchi; Melone
Annali di Chimica (Rome, Italy), 1959 , vol. 49, p. 1192,1203
反应条件
1.5 Au/TiO2 in dichloromethane
2 h; Photolysis;
参考文献
Neau, Tefan; Cojocaru, Bogdan; Parvulescu, Vasile I.; Omoghi, Vasile; Alvaro, Mercedes; Garcia, Hermenegildo
Journal of Materials Chemistry, 2010 , vol. 20, # 20 p. 4050 - 4054
