2-氨基-5-硝基苯磺酸合成路线 (共 20 条)
反应条件
[RuCl(P(C6H5)3)2(O(C6H4)NCH(C4H3N))]; sodium N-bromobenzenesulfonamide; sodium hydroxide in water; acetonitrile T=39.84°C; 5.75 h;
参考文献
Jagadeesh; Karthikeyan; Nithya; Sandhya, Y. Sree; Reddy, S. Sudhaker; Reddy, P. Pradeep Kumar; Kumar, M. Vinod; Charan, K.T. Prabhu; Narender; Bhagat
Journal of Molecular Catalysis A: Chemical, 2010 , vol. 328, # 1-2 p. 99 - 107
反应条件
dihydrogen peroxide in sodium hydroxide
反应条件
sulfuric acid; iodine T=140°C;
参考文献
Journal of the American Chemical Society, , vol. 43, p. 311
Journal of the Chemical Society, , vol. 117, p. 1407
Journal of the Indian Chemical Society, , vol. 4, p. 323
Chem. Zentralbl., , vol. 99, # I p. 491
反应条件
sodium nitrite in hydrogenchloride; water
反应条件
ammonia T=150°C; unter Druck;
参考文献
Grundlegende Operationen der Farbenchemie, 5. Aufl. <Wien 1943>, S. 96
反应条件
0.05 h; microwave irradiation;
参考文献
Kapoor; Srivastava, Pratibha; Singh, Gurdip; Froehlich, Roland
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2007 , vol. 46, # 8 p. 1283 - 1288
参考文献
Journal of the Chemical Society, , vol. 117, p. 1407
反应条件
1.1: trichlorophosphate / sulfolane / 80 - 120 °C 1.2: 10 - 95 °C 1.3: 25 - 80 °C / pH 6 - 8 2.1: hydrogen / palladium 10 on activated carbon / tetrahydrofuran; methanol / 23 °C / 2585.81 Torr / Industry scale; Autoclave View Scheme
参考文献
ANADYS PHARMACEUTICALS, INC.
Patent: WO2008/124450 A1, 2008 ;
参考文献
Datta; Varma
Journal of the Indian Chemical Society, 1927 , vol. 4, p. 323
Chem. Zentralbl., 1928 , vol. 99, # I p. 491
参考文献
Datta; Varma
Journal of the Indian Chemical Society, 1927 , vol. 4, p. 323
Chem. Zentralbl., 1928 , vol. 99, # I p. 491