7,9-二去羧基吡咯喹啉醌合成路线 （共 7 条）
反应条件
potassium carbonate
T=85°C; 24 h;
参考文献
Sleath,P.R.; Noar,J.B.; Eberlein,G.A.
Journal of the American Chemical Society, 1985 , vol. 107, p. 3328
反应条件
1: 97 percent / H2, HCl / Pd/C (10percent) / H2O / 1.5 h / 2280 Torr
3: 75 percent / K2CO3 (0.5M) / 24 h / 85 °C
View Scheme
参考文献
Sleath,P.R.; Noar,J.B.; Eberlein,G.A.
Journal of the American Chemical Society, 1985 , vol. 107, p. 3328
反应条件
potassium carbonate
T=60°C; 5 h;
参考文献
Itoh; Kato -i.; Inoue; Kitamura; Komatsu; Ohshiro
Synthesis, 1987 , # 12 p. 1067 - 1071
反应条件
2: 75 percent / K2CO3 (0.5M) / 24 h / 85 °C
View Scheme
参考文献
Sleath,P.R.; Noar,J.B.; Eberlein,G.A.
Journal of the American Chemical Society, 1985 , vol. 107, p. 3328
反应条件
1: 94 percent / nitrobenzene / 1 h / Heating
2: 71 percent / ceric ammonium nitrate / acetonitrile; H2O / 0.17 h / 0 °C
3: 100 percent / aq. K2CO3 / 5 h / 60 °C
View Scheme
参考文献
Itoh; Kato -i.; Inoue; Kitamura; Komatsu; Ohshiro
Synthesis, 1987 , # 12 p. 1067 - 1071
反应条件
1: 71 percent / ceric ammonium nitrate / acetonitrile; H2O / 0.17 h / 0 °C
2: 100 percent / aq. K2CO3 / 5 h / 60 °C
View Scheme
参考文献
Itoh; Kato -i.; Inoue; Kitamura; Komatsu; Ohshiro
Synthesis, 1987 , # 12 p. 1067 - 1071
反应条件
1: 94 percent / aq. K2CO3 / acetonitrile / 2 h / Ambient temperature
2: 94 percent / nitrobenzene / 1 h / Heating
3: 71 percent / ceric ammonium nitrate / acetonitrile; H2O / 0.17 h / 0 °C
4: 100 percent / aq. K2CO3 / 5 h / 60 °C
View Scheme
参考文献
Itoh; Kato -i.; Inoue; Kitamura; Komatsu; Ohshiro
Synthesis, 1987 , # 12 p. 1067 - 1071
