(Z)-1,4-二苯基-2-丁烯-1,4-二酮合成路线 （共 65 条）
反应条件
gold in 1,2-dichloro-ethane
T=60°C; 24 h;
参考文献
Zhou, Yibo; Trewyn, Brian G.; Angelici, Robert J.; Woo, L. Keith
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11734 - 11743
反应条件
gold in 1,2-dichloro-ethane
T=60°C; 24 h;
参考文献
Zhou, Yibo; Trewyn, Brian G.; Angelici, Robert J.; Woo, L. Keith
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11734 - 11743
反应条件
gold in 1,2-dichloro-ethane
T=60°C; 24 h;
参考文献
Zhou, Yibo; Trewyn, Brian G.; Angelici, Robert J.; Woo, L. Keith
Journal of the American Chemical Society, 2009 , vol. 131, # 33 p. 11734 - 11743
反应条件
1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in water; acetonitrile
T=28°C; 8 h; Inert atmosphere;
参考文献
Jadhav, Appaso Mahadev; Gawade, Sagar Ashok; Vasu, Dhananjayan; Dateer, Ramesh B.; Liu, Rai-Shung
Chemistry - A European Journal, 2014 , vol. 20, # 7 p. 1813 - 1817
反应条件
1: BF3*OEt2 / tetrahydrofuran / -78 °C
2: 59 percent / o-iodoxybenzoic acid / dimethylsulfoxide / 20 h / 20 °C
View Scheme
参考文献
Crone, Benedikt; Kirsch, Stefan F.
Chemical Communications, 2006 , # 7 p. 764 - 766
反应条件
1: BF3*OEt2 / tetrahydrofuran / -78 °C
2: 59 percent / o-iodoxybenzoic acid / dimethylsulfoxide / 20 h / 20 °C
View Scheme
参考文献
Crone, Benedikt; Kirsch, Stefan F.
Chemical Communications, 2006 , # 7 p. 764 - 766
反应条件
oxygen; gold
T=60°C; P=760.051 Torr; 29 h; optical yield given as percent de;
参考文献
Zhou, Yibo; Angelici, Robert J.; Keith Woo
Catalysis Letters, 2010 , vol. 137, # 1-2 p. 8 - 15
反应条件
1: iodine; copper(ll) bromide / N,N-dimethyl-formamide / 20 h / 80 °C / |Sealed tube
2: hexane; ethyl acetate / 5 h / 20 °C / |Irradiation
View Scheme
参考文献
Xu, Kun; Fang, Yang; Yan, Zicong; Zha, Zhenggen; Wang, Zhiyong
Organic Letters, 2013 , vol. 15, # 9 p. 2148 - 2151
反应条件
1: iodine; copper(ll) bromide / N,N-dimethyl-formamide / 20 h / 80 °C / |Sealed tube
2: hexane; ethyl acetate / 5 h / 20 °C / |Irradiation
View Scheme
参考文献
Xu, Kun; Fang, Yang; Yan, Zicong; Zha, Zhenggen; Wang, Zhiyong
Organic Letters, 2013 , vol. 15, # 9 p. 2148 - 2151
反应条件
1: iodine; copper(ll) bromide / N,N-dimethyl-formamide / 20 h / 80 °C / |Sealed tube
2: hexane; ethyl acetate / 5 h / 20 °C / |Irradiation
View Scheme
参考文献
Xu, Kun; Fang, Yang; Yan, Zicong; Zha, Zhenggen; Wang, Zhiyong
Organic Letters, 2013 , vol. 15, # 9 p. 2148 - 2151
