对苯二甲酸双(2-羟乙基)酯合成路线 (共 16 条)
反应条件
potassium tert-butylate; (1,3-biphenyl)imidazolinium chloride in tetrahydrofuran 0.5 h;
参考文献
Organic Letters, , vol. 4, # 21 p. 3587 - 3590
反应条件
1: Deloxan ASP I/7 T=250°C; P=760.051 Torr; 2: ethylene glycol With sodium hydroxide T=220°C; P=1125.11 Torr; 3: With cation exchange resin "AMBERLITE IR-120B"; anion exchange resin "AMBERLITE IRA96SB"; cation exchange resin "AMBERLITE IR-120B" Product distribution / selectivity; more than 3 stages;
参考文献
EP1510514 A1, ;
Page/Page column 15-27 ;
反应条件
1: Deloxan ASP I/7; polymethaxylylene adipamide T=250°C; P=760.051 Torr; 2: ethylene glycol With sodium hydroxide T=220°C; P=975.098 Torr; 3: With cation exchange resin "AMBERLITE IR-120B"; anion exchange resin "AMBERLITE IRA96SB"; cation exchange resin "AMBERLITE IR-120B" Product distribution / selectivity; more than 3 stages;
参考文献
EP1510514 A1, ;
Page/Page column 29-31 ;
参考文献
US2005/255139 A1, ;
Page/Page column 8 ;
反应条件
potassium carbonate T=185°C; 4 h; Product distribution / selectivity;
参考文献
US2009/133200 A1, ;
Page/Page column 6-8 ;
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene T=190°C; 0.108333 h; Product distribution / selectivity;
参考文献
US2012/223270 A1, ;
Page/Page column 8 ;
反应条件
1: Deloxan ASP I/7 T=280°C; 2: ethylene glycol With sodium hydroxide T=220°C; Product distribution / selectivity;
参考文献
EP1510514 A1, ;
Page/Page column 28 ;
反应条件
zinc diacetate; chloroacetic acid T=70°C; 24 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 82, # 1-4 p. 109 - 116
反应条件
1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine 24 h; Product distribution / selectivity;
参考文献
US2012/223270 A1, ;
Page/Page column 15 ;