4,4'-二甲氧基硫代二苯甲酮合成路线 （共 53 条）
参考文献
Helvetica Chimica Acta, , vol. 3, p. 838
反应条件
NSC26899; bis(trifluoroacetato)-1,2-phenylenedimercury in acetonitrile
T=25°C; 0.25 h;
参考文献
Wuest, James D.; Zacharie; Boulos
Journal of the American Chemical Society, 1985 , vol. 107, # 21 p. 6121 - 6123
反应条件
aluminum oxide; NaBEt3H; iron(II) chloride in tetrahydrofuran; benzene
Ambient temperature;
参考文献
Alper, Howard; Ripley, Sharon; Prince, Trish L.
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 250 - 252
反应条件
NaBEt3H; iron(II) chloride in tetrahydrofuran
1.) -78 deg C, 10 min.; 2.) room temp.;
参考文献
Alper, Howard; Ripley, Sharon; Prince, Trish L.
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 250 - 252
反应条件
1: diethyl ether
2: diethyl ether
View Scheme
参考文献
Bergmann; Wagenberg
Chemische Berichte, 1930 , vol. 63, p. 2585,2589
反应条件
Eindampfen bei Normaldruck in der Waerme;
参考文献
Bergmann; Wagenberg
Chemische Berichte, 1930 , vol. 63, p. 2585,2589
参考文献
Schoenberg
Chemische Berichte, 1925 , vol. 58, p. 1801
反应条件
in tetrahydrofuran
T=-40 - -20°C; Elimination; cycloaddition; 4 h;
参考文献
Huisgen, Rolf; Li, Xingya; Mloston, Grzegorz; Fulka, Claudia
European Journal of Organic Chemistry, 2000 , # 9 p. 1695 - 1702
反应条件
in tetrahydrofuran
T=-45°C;
参考文献
Xingya, Li; Huisgen, Rolf
Tetrahedron Letters, 1983 , vol. 24, # 39 p. 4181 - 4184
反应条件
1: -78 °C
2: -45 °C
3: 95 percent / tetrahydrofuran / -45 °C
View Scheme
参考文献
Xingya, Li; Huisgen, Rolf
Tetrahedron Letters, 1983 , vol. 24, # 39 p. 4181 - 4184
